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HH-Caproic acid填充柱 己酸的纯度测定
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HH-Caproic acid填充柱 己酸的纯度测定

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产品名称:HH-Caproic acid填充柱 己酸的纯度测定

产品型号:HH-Caproic acid填充柱

产品厂商:浩瀚色谱(山东)应用技术开发有限公司

简单介绍

己酸的纯度测定,液化石油气,二甲醚,甲缩醛,乙缩醛,乙醇,室内空气,焦炉煤气,炼厂气,天然气,变压器油,多氯联苯,植物油,6号溶剂残留,裂解进样器,消毒剂,氨水,乙缩醛

HH-Caproic acid填充柱 己酸的纯度测定的详细介绍

己酸的纯度测定
己酸的纯度测定 详细信息:

名称:填充柱
规格:2m*3mm
型号:HH-Caproic acid
应用:己酸的纯度测定


对己酸新的合成工艺进行了探讨。采用二步法制备已酸,以2-辛醇为反应原料,2-辛醇气相脱水得到2-辛烯,再氧化2-辛烯为已酸的合成工艺路线;研究了负载型脱水催化剂对2-辛醇气相脱水合成2-辛烯的催化作用,由固定床反应器考察了其催化性能;用XRD、BET等手段对催化剂进行表征,研究其可能的反应机理,并对催化剂的失活原因进行了考察;以过氧化氢为氧化剂,磷钨酸为催化剂,十六烷基吡啶为相转移催化剂催化氧化2-辛烯制备已酸;分别考察了反应温度、反应时间、催化剂的物质的量对已酸收率的影响;研究了反应控制相转移催化剂的反应机理,因为催化剂能回收,这种氧化2-辛烯为已酸的合成方法更加环境友好和经济性。

滕州市浩瀚色谱仪器技术服务有限公司,研发专用填充柱测定己酸的纯度,杂质空气,水分,辛醇和己酸得到有效分离,面积归一法定量,结果准确。

己酸的纯度测定 测试谱图:



Purity determination of caproic acid
Determination of the purity of hexanoic acid Details:

Name: Packed column
Specification: 2m*3mm
Model: HH-Caproic acid
Application: Purity determination of caproic acid


The new synthetic process of caproic acid was discussed. A two-step method was used to prepare hexanoic acid, with 2-octanol as the reaction raw material, 2-octanol gas-phase dehydration to obtain 2-octene, and 2-octene reoxidation as the synthesis process of hexanoic acid; The catalytic performance of 2-octanol gas-phase dehydration to 2-octene was investigated by a fixed bed reactor; the catalyst was characterized by XRD, BET and other means, and its possible reaction mechanism was studied, and the catalyst was deactivated The reasons were investigated; hydrogen peroxide was used as the oxidant, phosphotungstic acid was used as the catalyst, and cetylpyridine was used as the phase transfer catalyst to catalyze the oxidation of 2-octene to hexanoic acid; the reaction temperature, reaction time, and the catalyst material were investigated separately The influence of the amount on the yield of hexanoic acid; the reaction mechanism of the reaction control phase transfer catalyst is studied. Because the catalyst can be recycled, the synthesis method of oxidizing 2-octene to hexanoic acid is more environmentally friendly and economical.

Tengzhou Haohan Chromatography Instrument Technology Service Co., Ltd. has developed a special packed column to determine the purity of caproic acid. Impurity air, moisture, octanol and caproic acid are effectively separated, and the area normalization method is quantified, and the result is accurate and reliable.

Purity determination of caproic acid Test spectrum:

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